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<title>UTas ePrints - Bis[tris(1-methyl-1H-imidazol-2-yl)phosphine-3N3]iron(II) tetrachloroferrate(II) methanol tetrasolvate (ca 153 K) and bis[tris(1-methyl-1H-imidazol-2-yl)methanol-3N3]iron(III) bis[tetrachloroferrate(III)] chloride (redetermination, ca 153 K)</title>
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<meta content="Batten, M. P." name="eprints.creators_name" />
<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Cavell, K. J." name="eprints.creators_name" />
<meta content="Ruther, T." name="eprints.creators_name" />
<meta content="Skelton, B.W." name="eprints.creators_name" />
<meta content="White, A.H." name="eprints.creators_name" />
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<meta content="allan.canty@utas.edu.au" name="eprints.creators_id" />
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<meta content="2007-12-21 03:35:13" name="eprints.datestamp" />
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<meta content="Bis[tris(1-methyl-1H-imidazol-2-yl)phosphine-3N3]iron(II)
tetrachloroferrate(II) methanol tetrasolvate (ca 153 K) and
bis[tris(1-methyl-1H-imidazol-2-yl)methanol-3N3]iron(III)
bis[tetrachloroferrate(III)] chloride (redetermination, ca 153 K)" name="eprints.title" />
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<meta content="250201" name="eprints.subjects" />
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<meta content="The ®rst of the title compounds, [Fe(C12H15N6P)2][FeCl4]-
4CH4O, is the ®rst homoleptic bis(ligand)iron(II) species
reported for this phosphorus bridgehead ligand; interestingly, the complex is isomorphous with its tris(1-methyl-1H-imidazol-2-yl)methanol counterpart, the second of the title compounds, [Fe(C13H16N6O)2][FeCl4]2Cl. In both compounds, the Fe atom of the cation lies on an inversion centre. The structure determinations presented here allow an interesting comparison of iron(II) and iron(III) species in similar coordination environments." name="eprints.abstract" />
<meta content="2004" name="eprints.date" />
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<meta content="Acta Crystallographica Section C" name="eprints.publication" />
<meta content="C60" name="eprints.volume" />
<meta content="m311-m313" name="eprints.pagerange" />
<meta content="10.1107/S0108270104010893" name="eprints.id_number" />
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<meta content="http://dx.doi.org/10.1107/S0108270104010893" name="eprints.official_url" />
<meta content="Anderson, P. A., Astley, T., Hitchman, M. A., Keene, F. R., Moubaraki, B.,
Murray, K. S., Skelton, B. W., Tiekink, E. R. T., Toftlund, H. & White, A. H.
(2000). J. Chem. Soc. Dalton Trans. pp. 3505±3512.
Chauvin, A.-S., Frapart, Y.-M., Vaissermann, J., Donnadieu, B., Tuchagues,
J.-P., Chottard, J.-C. & Li, Y. (2003). Inorg. Chem. 42, 1895±1900.
Hall, S. R., King, G. S. D. & Stewart, J. M. (1995). The Xtal3.5 User's Manual.
University of Western Australia: Lamb, Perth.
Reger, D. L., Little, C. A., Rheingold, A. L., Lam, M., Concolino, T., Mohan,
A. & Long, G. J. (2000). Inorg. Chem. 39, 4674±4675.
Sheldrick, G. M. (1996). SADABS. University of GoÈ ttingen, Germany.
Siemens (1995). SMART and SAINT. Siemens Analytical X-ray Instruments
Inc., Madison, Wisconsin, USA.
Wu, F.-J., Kurtz, D. M. Jr, Hagen, K. S., Nyman, P. D., Debrunner, P. G. &
Vankai, V. A. (1990). Inorg. Chem. 29, 5174±5183.
Wu, L. P., Yamagiwa, Y., Ino, I., Sugimoto, K., Kuroda-Sowa, T., Kamikawa, T.
& Munakata, M. (1999). Polyhedron, 18, 2047±2053.
A" name="eprints.referencetext" />
<meta content="Batten, M. P. and Canty, A.J. and Cavell, K. J. and Ruther, T. and Skelton, B.W. and White, A.H. (2004) Bis[tris(1-methyl-1H-imidazol-2-yl)phosphine-3N3]iron(II) tetrachloroferrate(II) methanol tetrasolvate (ca 153 K) and bis[tris(1-methyl-1H-imidazol-2-yl)methanol-3N3]iron(III) bis[tetrachloroferrate(III)] chloride (redetermination, ca 153 K). Acta Crystallographica Section C, C60 . m311-m313. ISSN 0108-2701" name="eprints.citation" />
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tetrachloroferrate(II) methanol tetrasolvate (ca 153 K) and
bis[tris(1-methyl-1H-imidazol-2-yl)methanol-3N3]iron(III)
bis[tetrachloroferrate(III)] chloride (redetermination, ca 153 K)" name="DC.title" />
<meta content="Batten, M. P." name="DC.creator" />
<meta content="Canty, A.J." name="DC.creator" />
<meta content="Cavell, K. J." name="DC.creator" />
<meta content="Ruther, T." name="DC.creator" />
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<meta content="The ®rst of the title compounds, [Fe(C12H15N6P)2][FeCl4]-
4CH4O, is the ®rst homoleptic bis(ligand)iron(II) species
reported for this phosphorus bridgehead ligand; interestingly, the complex is isomorphous with its tris(1-methyl-1H-imidazol-2-yl)methanol counterpart, the second of the title compounds, [Fe(C13H16N6O)2][FeCl4]2Cl. In both compounds, the Fe atom of the cation lies on an inversion centre. The structure determinations presented here allow an interesting comparison of iron(II) and iron(III) species in similar coordination environments." name="DC.description" />
<meta content="2004" name="DC.date" />
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<h1 class="ep_tm_pagetitle">Bis[tris(1-methyl-1H-imidazol-2-yl)phosphine-3N3]iron(II) tetrachloroferrate(II) methanol tetrasolvate (ca 153 K) and bis[tris(1-methyl-1H-imidazol-2-yl)methanol-3N3]iron(III) bis[tetrachloroferrate(III)] chloride (redetermination, ca 153 K)</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Batten, M. P.</span> and <span class="person_name">Canty, A.J.</span> and <span class="person_name">Cavell, K. J.</span> and <span class="person_name">Ruther, T.</span> and <span class="person_name">Skelton, B.W.</span> and <span class="person_name">White, A.H.</span> (2004) <xhtml:em>Bis[tris(1-methyl-1H-imidazol-2-yl)phosphine-3N3]iron(II) tetrachloroferrate(II) methanol tetrasolvate (ca 153 K) and bis[tris(1-methyl-1H-imidazol-2-yl)methanol-3N3]iron(III) bis[tetrachloroferrate(III)] chloride (redetermination, ca 153 K).</xhtml:em> Acta Crystallographica Section C, C60 . m311-m313. ISSN 0108-2701</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2783/1/AC_2C_C60_2C_m311.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" border="0" class="ep_doc_icon" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2783/1/AC_2C_C60_2C_m311.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />280Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input value="3689" name="docid" accept-charset="utf-8" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1107/S0108270104010893">http://dx.doi.org/10.1107/S0108270104010893</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The ®rst of the title compounds, [Fe(C12H15N6P)2][FeCl4]-
4CH4O, is the ®rst homoleptic bis(ligand)iron(II) species
reported for this phosphorus bridgehead ligand; interestingly, the complex is isomorphous with its tris(1-methyl-1H-imidazol-2-yl)methanol counterpart, the second of the title compounds, [Fe(C13H16N6O)2][FeCl4]2Cl. In both compounds, the Fe atom of the cation lies on an inversion centre. The structure determinations presented here allow an interesting comparison of iron(II) and iron(III) species in similar coordination environments.</p></div><table style="margin-bottom: 1em" border="0" cellpadding="3" class="not_ep_block"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Additional Information:</th><td valign="top" class="ep_row">"The definitive version is available at www.blackwell-synergy.com"
</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/250201.html">250000 Chemical Sciences > 250200 Inorganic Chemistry > 250201 Transition Metal Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2783</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">21 Dec 2007 14:35</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">01 Feb 2008 14:14</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2783;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2783">item control page</a></p>
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